Phosphorus NMR analysis of phospholipids in detergents.
نویسندگان
چکیده
منابع مشابه
Phosphorus NMR analysis of phospholipids in detergents.
Various detergents can be used to dissolve phospholipids, resulting in very narrow 31PNMR resonances. The resonances are well resolved, allowing identification and quantitative analysis of phospholipids in a mixture. The chemical shift depends strongly on pH, reflecting changes in the state of ionization of the phospholipid headgroup moieties. Samples of phospholipids dissolved in aqueous deter...
متن کاملSlow-Motional NMR Line Shapes for Very Anisotropic Rotational Diffusion. Phosphorus-31 NMR of Phospholipids
The model of Mason, Polnaszek, and Freed for ESR-slow-tumbling spectra is extended to the case of NMR line shapes for arbitrary tilt of the internal axis of relatively rapid rotation with respect to the principal axes of the chemical shielding tensor for a decoupled I = 1 / 2 nucleus. The theory is applied to an analysis of 31P NMR spectra from partially hydrated dipalmitoylphosphatidylcholine ...
متن کاملQuantitative analysis of phospholipids by 31P-NMR.
High-field 31P nuclear magnetic resonance spectroscopy was used to quantitate phospholipids in mixtures in organic solvents. The sample is dissolved in chloroform-methanol and analyzed at 161.7 MHz with decoupling of the protons. Signals were identified using authentic compounds, and their relative distribution was measured in mole percent. The method has good accuracy and reproducibility, and ...
متن کاملanalysis of power in the network society
اندیشمندان و صاحب نظران علوم اجتماعی بر این باورند که مرحله تازه ای در تاریخ جوامع بشری اغاز شده است. ویژگیهای این جامعه نو را می توان پدیده هایی از جمله اقتصاد اطلاعاتی جهانی ، هندسه متغیر شبکه ای، فرهنگ مجاز واقعی ، توسعه حیرت انگیز فناوری های دیجیتال، خدمات پیوسته و نیز فشردگی زمان و مکان برشمرد. از سوی دیگر قدرت به عنوان موضوع اصلی علم سیاست جایگاه مهمی در روابط انسانی دارد، قدرت و بازتولید...
15 صفحه اولNmr of Phospholipids in Postmortem Schizophrenic Brains
It has been hypothesized that schizophrenia arises from cell membrane abnormalities due to changes in phospholipid (PL) composition. Studies on erythrocytes and platelets suggest that alterations in membrane PL composition play a role in schizophrenia. It is essential to measure PL composition in the brain itself, which typically is only possible postmortem. In vivo P NMR of PL precursors and d...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of Lipid Research
سال: 1979
ISSN: 0022-2275
DOI: 10.1016/s0022-2275(20)40624-8